The exquisite pleasure derived from smelling fragrant flowers would almost instinctively induce man to attempt to separate the odoriferous principle from them, so as to have the perfume when the season denies the flowers. Thus we find the alchemists of old, torturing the plants in every way their invention could devise for this end; and it is on their experiments that the whole art of perfumery has been reared. Without recapitulating those facts which may be found diffused through nearly all the old authors on medical botany, chemistry, pharmacy, and works of this character, from the time of Paracelsus to Celnart, we may state at once the mode of operation adopted by the practical perfumer of the present day for preparing the various extracts or essences, waters, oils, pomades, &c., used in his calling.
The processes are divided into four distinct operations; viz.—
1. Expression; 2. Distillation; 3. Maceration; 4. Absorption.
1. Expression is only adopted where the plant is very prolific in its volatile or essential oil,—i.e. its odor; such, for instance, as is found in the pellicle or outer peel of the orange, lemon, and citron, and a few others. In these cases, the parts of the plant containing the odoriferous principle are put sometimes in a cloth bag, and at others by themselves into a press, and by mere mechanical force it is squeezed out. The press is an iron vessel of immense strength, varying in size from six inches in diameter, and twelve deep, and upwards, to contain one hundred weight or more; it has a small aperture at the bottom to allow the expressed material to run for collection; in the interior is placed a perforated false bottom, and on this the substance to be squeezed is placed, covered with an iron plate fitting the interior; this is connected with a powerful screw, which, being turned, forces the substance so closely together, that the little vessels containing the essential oils are burst, and it thus escapes. The common tincture press is indeed a model of such an instrument. The oils which are thus collected are contaminated with watery extracts, which exudes at the same time, and from which it has to be separated; this it does by itself in a measure, by standing in a quiet place, and it is then poured off and strained.
[Illustration: Pipette to draw off small portions of otto from water.]
2. Distillation.—The plant, or part of it, which contains the odoriferous principle, is placed in an iron, copper, or glass pan, varying in size from that capable of holding from one to twenty gallons, and covered with water; to the pan a dome-shaped lid is fitted, terminating with a pipe, which is twisted corkscrew fashion, and fixed in a bucket, with the end peeping out like a tap in a barrel. The water in the still—for such is the name of the apparatus—is made to boil; and having no other exit, the steam must pass through the coiled